The purpose of this study was to investigate the application method of S-P Chart and the difference of appreciation level received after treatment. Hopefully, it could provide guidelines for the improvement of evaluation program for elementary and secondary school. The study adopted the approach of action research, searched the procedures f or the design, interpretation, and judgement of S-P Chart, while by the use of Semantic Differential Method, attempted to understand the differences of appreciation level received. It was found that S-P Chart's use in analyzing the curve of gained points, together with correct response rate, could early predict the specific students who needed help. By the use of the results of S D Method showed poesitive confirmation of the acceptance level. On every item and on the whole, all reached statistical significance level. The subjects of this study, after 10 sessions of study and pratice, could complete the drawing, interpreting, and judging of S-P Chart, and in the mean while, applying it in learning diagnosis. In the future, there are needed research in: (1) formulation of S-P Chart theory, and (2) application of S-P Chart in obtaining various evaluative data. The author shall continue to further studies in these two areas.