In a coastal forest restoration project supported by Kenting National Park charcoal were made from burnt wood of Leucaena leucocephala for conservation of natural resource and utilization of alien invasive species. A traditional earthen kiln was used to make the charcoal. The temperatures of the carbonization and chimney in the kiln were monitored using K-type thermocouple and the yields were recorded. Charcoals, taken from various vertical positions in the kiln, were sampled to study properties such as electric resistivity, pH, carbon content, true density and specific surface area, and yield to understand the effects of temperature on carbonization. The results showed that carbonization temperature at the upper part of the kiln increased more rapidly than that at the lower part of the kiln. The highest temperature of the upper part in the kiln at the end of carbonization was slightly above 750oC. The yield of leucaena wood charcoal averaged 29.97%. The electric resistivity of charcoal samples decreased substantially with increasing carbonization temperature. The pH of leucaena wood charcoal ranged from of 9.3 to 9.80 and was independent of carbonization temperatures. The carbon content, true density, and specific surface area of charcoal rose with increasing temperature. The carbon conservation was 46.10%.