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題名：微波消化萃取配合快速原子撞擊同位素稀釋質譜法分析頭髮中之安非他命
書刊名：警學叢刊
作者：王勝盟／雷逸智／蔡麗琴／姜雲生／凌永健
作者(外文)：Wang, Sheng Meng／Lei, Yi Chin／Tsai, Li Chin／Giang, Yun Seng／Ling, Yong Chein
出版日期：1997
卷期：28:1=113
頁次：頁85-105
主題關鍵詞：微波消化萃取；快速原子撞擊質譜法；頭髮分析；安非他命；甲基安非他命
原始連結：連回原系統網址new window
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  • 被引用次數被引用次數:期刊(0) 博士論文(0) 專書(0) 專書論文(0)
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  • 點閱點閱:121
　　　　　鑒於傳統上以酸鹼或酵素消化、萃取頭髮中之待析物需要花費冗長的時間，步驟 亦繁雜，本研究乃試圖發展一種快速、方便、可行的前處理及儀器分析方法。以微波消化萃 取配合快速原子撞擊同位素稀釋質譜法分析頭髮中之安非他命及甲基安非他命具有樣品製備 容易、分析快速、再現性佳、靈敏度好、適合於分析不易揮發、遇熱不穩定、高極性化合物 等優點。 　　本法之方法偵測極限對安非他命為0.006ppm，對甲基安非他命為0.009ppm。檢量線的線 性範圍在0.01ppm至10.0ppm之間，線性相關係數對安非他命為0.997，對甲基安非他命為 0.998。樣品在各種濃度不同時間的七次重複分析中，其變異係數均在10%以下，在真實樣品 的分析方面，先以快速原子撞擊--磁場（電場聯結掃描法進行定性掃描，若含有待析物之離 子譜峰時（即呈陽性反應），再以快速原子撞 擊--選擇離子偵測法做定量分析，並與傳統 之固相萃取--氣相層析╱質譜法做一比較。
期刊論文
1.Nakahara, Y.、Takahashi, K.、Shimamine, M.、Takeda, Y.(1991)。Hair analysis for drug abuse: I. Determination of methamphetamine and amphetamine in hair by stable isotope dilution gas chromatography/mass spectrometry method。Journal of Forensic Sciences，36(1)，70-78。  new window
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3.Nakahara, Y.、Shimamine, M.、Takahashi, K.(1992)。Hair analysis for drugs of abuse. III. movement and stability of methoxyphenamine (as a model compound of methamphetamine) along hair shaft with hair growth。Journal of Analytical Toxicology，16(4)，253-257。  new window
4.Welch, M. J.、Sniegoski, L. T.、Aligood, C. C.、Habram, M.(1993)。Hair analysis for drugs of abuse: evaluation of analytical methods, environmental issues, and development of reference materials。Journal of Analytical Toxicology，17(7)，389-398。  new window
5.Moeller, M. R.、Fey, P.、Wening, R.(1993)。Simultaneous determination of drugs of abuse (opiates, cocaine and amphetamine) human hair by GC/MS and its application to a methadone treatment program。Forensic Science International，63(1-3)，185-206。  new window
6.Kintz, P.、Mangin, P.(1993)。Determination of gestational opiate, nicotine, benzodiazepine, cocaine and amphetamine exposure by hair analysis。Journal of the Forensic Science Society，33(3)，139-142。  new window
7.Baumgartner, W. A.、Hill, V. A.、Blahd, W. H.(1989)。Hair analysis for drugs of abuse。Journal of Forensic Sciences，34(6)，1433-1453。  new window
8.Nakahara, Y.、Takahashi, K.、Konuma, K.(1993)。Hair analysis for drugs of abuse, VI. The excretion of methoxyphenamine and methamphetamine into beards of human subjects。Forensic Science International，63(1-3)，109-119。  new window
9.Ishiyama, I.、Nagai, T.、Toshida, S.(1983)。Detection of basic drugs from human hair。Journal of Forensic Sciences，28，380-385。  new window
10.Niwaguchi, T.、Suzuki, S.、Iuone, T.(1983)。Determination of methamphetamine in hair after single and repeated administration to rat。Archives of Toxicology，52(2)，157-164。  new window
11.Suzuki, O.、Hattori, H.、Asano, M.(1983)。Nails as useful materials for detection of methamphetamine or amphetamine abuse。Forensic Science International，24(1)，9-16。  new window
12.Suzuki, O.、Hattori, H.、Asano, M.(1984)。Detection of methamphetamine and amphetamine in a single human hair by GC/MS。Journal of Forensic Sciences，29(2)，611-617。  new window
13.Suzuki, S.、Inoue, T.、Hori, H.、Inayama, S.(1989)。Analysis of methamphetamine in hair, nail, sweat and saliva by mass fragmentography。Journal of Analytical Toxicology，13，176-178。  new window
14.Kintz, P.、Ludes, B.、Mangin, P.(1992)。Detection of drugs in human hair using Abbott ADx with confirmation by gas chromatography/mass spectrometry(GC/MS)。Journal of Forensic Sciences，37(1)，328-311。  new window
15.Barber, M.、Bordoli, R. S.、Sedgwick, R. D.、Tyler, A. N.(1981)。Fast atom bombardment of solids as an ion source in mass spectrometry。Nature，293，270-275。  new window
16.Arisz, P. W.、Kauw, H. J. J.、Boon, J. J.(1995)。Substituent distribution along the cellulose backbone in o-methylcelluloses using GC and FAB-MS for monomer and oligomer analysis。Carbohydrate Research，271(1)，1-14。  new window
17.Edwards, D. M. F.、Selva, E.、Stella, S.、Zerilli, L. F.、Gallo, G. G.(1992)。Mass spectrometric techniques for structure and novelty determination of kirromycin-like antibiotics。Biological Mass Spectrometry，21(1)，51-59。  new window
18.Saraswathi, M.、Miller, J. M.(1996)。A study of metal chelation of dinucleotide analogs in the gas-phase by fast-atom-bombardment mass-spectrometry。Journal of the American Society for Mass Spectrometry，7(1)，42-49。  new window
19.Davoli, E.、Fanelli, R.、Bagnati, R.(1993)。Purification and analysis of drug residues in urine samples by on-line immunoaffmity chromatography/high-performance liquid chromatography/continuous flow fast atom bombardment mass spectrometry。Analytical Chemistry，65(19)，2679-2685。  new window
20.Kemp, T. J.、Read, P. A.(1996)。Fast-atom-bombardment studies or amino-acid and peptide complexes of the uranyl-ion-ligand attachment, dissociation and fragmentation。Inorganica Chimica Acta，241(2)，105-110。  new window
21.Deterding, L. J.、Moseley, M. A.、Tomer, K. B.、Jorgenson, J. W.(1989)。Coaxial continuous flow fast atom bombardment in conjunction with tandem mass spectrometry for the analysis of biomolecules。Anal. Chem.，61(22)，2504-2511。  new window
22.Claydon, M. A.、Gordon, D. B.、Garner, G. V.、Lord, G. A.(1995)。A partial sequence of an IgG light-chain using continuous-flow HPLC-FAB mass-spectroscopy。Biochemical Society Transactions，23(4)，633-633。  new window
23.Price, K. R.、Eagles, J.、Fenwick, G. R.(1988)。Saponin composition of 13 varieties of legume seed using fast atom bombardment mass spectrometry。Journal Science of Food and Agriculture，42(2)，183-193。  new window
24.Fujiwara, H.、Chott, R. C.、Solsten, R. T.(1992)。Utility of liquid chromatography/fast atom bombardment mass spectrometry and liquid chromatography/thermospray mass spectrometry for structure identification of metabolites of a fluorinated herbicide。Biological Mass Spectrometry，21(9)，431-440。  new window
25.Onisko, B. C.、Barnes, J. P.、Staub, R. E.、Walker, F. H.、Kerlinger, N.(1991)。Metabolism of cycloate in radish leaf: Metabolite identification by packed capillary flow fast atom bombardment tandem mass spectrometry。Biological Mass Spectrometry，23(10)，626-636。  new window
26.Kishore, K.、Ganesh, K.(1993)。Synthesis, characterization, and thermal degradation studies on group VIA derived weak-link polymers。Macromolecules，26(17)，4700-4705。  new window
27.Zhou, X. F.、Peng, Z. H.、Geise, H. J.、Peng, B. X.、Li, Z. X.、Yan, M.、Dommisse, R.、Carleer, R.、Claeys, M.(1995)。Blue sensitizing dyes: synthesis, spectroscopy, and performance in photographic emulsions。Journal of Imaging Science and Technology，39(3)，244-252。  new window
28.Ventura, F.、Caixach, J.、Romero, J.、Espadaler, I.、Rivera, J.(1992)。New methods for the identification of surfactants and their acidic metabolites in raw and drinking water: FAB-MS and MS/MS。Water Science and Technology，25(11)，257-264。  new window
29.Florencio, M. H.、Duarte, M. F.、Bettencourt, A.(1995)。Optimization of fast-atombombardment (FAB) mass-spectra of arsenobetaine and arsenocholine。Applied Organometallic Chemistry，9(8)，719-720。  new window
30.Martins, L. M. D. R. S.、Dasilva, M. F. C. G.、Marques, I.、Dasilva, J. J. R. F.、Vaz, M. C. N.、Pombeiro, A. L. J.(1996)。Fast-atom-bombardment (FAB) mass-spectra of nitrile or cyanamide complexes with the (M(pH(2)Pch(2)CH(2)Pph(2))(2))(N+)(M=Fe or Re) metal sites - application to reactions induced under fab conditions。Rapid communications in mass spectrometry，10(4)，447-454。  new window
31.Ohnishi-Kameyama, M.、Nagata, T.、Akiba, M.、Sasaki, Y.、Kakimoto, N.(1995)。Identification of organogermanium compounds as matrix complexes in fast-atom bombardment mass spectrometry。Rapid communication in mass spectrometry，9，877-882。  new window
32.Saraswathi, M.、Miller, J. M.(1995)。Fast-atom bombardment mass spectrometryy of 2, 4-diketonate complexes of transition metals [V(IIl), Cr(III), Mn(III), Fe(III), Co(III), Ru(III) and Os(III)]。Rapid communication in mass spectrometry，9，1101-1105。  new window
33.Henczi, M.、Weaver, D. F.(1995)。Fast-atom bombaredment mass spectrometry coupled with collision-induced dissociation of a hydantion series for fragmentation studies。Rapid communication in mass spectrometry，9，804-808。  new window
34.Boryak, O. A.、Koscvich, M. V.、Shelkovsky, V. S.、Blagoy, Y. P.(1995)。Study of watercryoprotecter mixtures by low temperature fast-atom bombardment mass spectrometry。Rapid communication in mass spectrometry，9，978-984。  new window
35.Thompson, W. C.、Dasgupta, A.(1994)。Microwave-induced rapid preparation of fluoroderivatives of amphetamine, methamphetamine, and 3,4-MDMA for GC/MS confirmation assays。Clinical Chemistry，40(9)，1703-1706。  new window
36.Franke, M.、Winek, C. L.、Kingston, H. M.(1996)。Extraction of selected drugs from serum using microwave irradiation。Forensic Science International，81(1)，51-59。  new window
37.David, B.(1988)。Rapid sample preparation for determination of iron in tissue by closed-vessel digestion and microwave energy。Clinical Chemistry，34(6)，1128-1130。  new window
38.Sturgeon, R.(1988)。Acid digestion of marine samples for trace element analysis using microwave heating。Analyst，113(1)，159-163。  new window
39.Baldwin, S.、Deaker, M.、Maher, W.(1994)。Low-volume microwave digestion of marine biological tissues for the measurement of trace elements。Analyst，119(8)，1701-1704。  new window
40.Chen, S. S.、Spiro, M.(1994)。Study of microwave extraction of essential oil constituents from plant materials。Journal of Microwave Power and Electromagnetic Energy，29(4)，231-241。  new window
41.Ganzler, K.、Bati, J.、Valko, K.(1986)。A novel sample preparation method for chromatography。Journal of Chromatography A，371，299-306。  new window
42.Ganzler, K.、Szinai, I.(1990)。Effective sample preparation method for extracting biologically active compounds from different matrices by a microwave technique。Journal of Chromatography A，520，257-262。  new window
43.Analytical Methods Committee(1987)。Recommendations for the definition, estimation and use of the detection limit。Analyst，112，199-204。  new window
學位論文
1.廖俊雄(1995)。超臨界二氧化碳流體萃取土壤中有機氯農藥分析方法之研究(碩士論文)。國立清華大學。  延伸查詢new window
2.雷逸智(1996)。質譜法直接分析及辨識材料吸附安非他命之研究(碩士論文)。國立清華大學。  延伸查詢new window
圖書
1.Dell, A.(1987)。FAB mass spectrometry of carbohydrates in advance in carbohydrate chemistry and biochemistry。London：Academic Press。  new window
2.Morris, H. R.、Taylor, G. W.、Panico, M.、Dell, A.、Etienne, A. T.、McDowell, R. A.、Judkins, M. B.(1982)。Methods in protein sequence analysis。Clifon, New Jersey：Human Press。  new window
圖書論文
1.何國榮(1992)。磁場式質譜儀之質譜／質譜分析法（高能碰撞引致裂解）。質譜分析術專輯。新竹市。  延伸查詢new window
2.曹汝祥(1992)。快速原子撞擊質譜技術及其應用。質譜分析術專輯。新竹市。  延伸查詢new window
3.Fujiwara, H.、Wratten, S. J.(1987)。Application of fast atom bombardment mass spectrometry to polar pesticides。Applications of new mass spectrometry techniques in pesticide chemistry。Canada：John Wiley & Sons, Inc。  new window
 
 
 
 
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