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題名:射擊前及射擊後發射火藥顆粒系統化分析之研究
書刊名:刑事科學
作者:孟憲輝余秋忠郭惠源
作者(外文):Meng, Hsien-huiYu, Chiou-chungKwo, Hui-yuan
出版日期:1997
卷期:44
頁次:頁15-33
主題關鍵詞:子彈火藥顆粒發射火藥
原始連結:連回原系統網址new window
相關次數:
  • 被引用次數被引用次數:期刊(6) 博士論文(0) 專書(0) 專書論文(0)
  • 排除自我引用排除自我引用:1
  • 共同引用共同引用:11
  • 點閱點閱:22
     本研究首先針對24種不同之子彈發射火葯進行系統化分析。分析方法包括:顯微 觀察、安定劑之薄層層析、硝化纖維及硝化甘油之薄層層析及硝化纖維之紅外吸收光譜測定 等。結果發現 24 種火葯均含安定劑二苯胺 (diphenylamine) 及 (或 ) 其硝化衍生物,其 中 11 種另含安定劑 ethyl centralite。20 種火葯為雙基火葯,含硝化纖維及硝化甘油 ; 另有 4 種為單基火葯, 僅含硝化纖維。 本研究另進行前述樣品中 5 種子彈及 Geco.32 子彈之近距離試射,從被射物表面採下射擊殘留火葯顆粒,以前述方法分析。 其中 4 種發 射後樣品之分析結果與未發射樣品之結果相同,1 種未發現安定劑,但含硝化纖維及硝化甘 油,另有 1 種因未能採得顆粒樣品, 而以棉擦樣品分析,未能發現任何安定劑、硝化纖維 、及硝化甘油成分。本方法方便、便宜、操作容易,準確性高、靈敏度尚佳。雖不能分析棉 擦樣品,但只需 l ~ 2 粒火葯顆粒即可供分析。 故可供為基右單位分析發射前及發射後火 葯顆粒之用。
期刊論文
1.孟憲輝(19920300)。論射擊殘跡有機成分之鑑析。刑事科學,33,19-28。new window  延伸查詢new window
2.Meng, Hsien-Hui、Caddy, Brian(1995)。Detection of N,N′-diphenyl-N,N′-diethylurea (ethyl centralite) in gunshot residues using high-performance liquid chromatography with fluorescence detection。Analyst,120,1759-1762。  new window
3.孟憲輝(19960300)。射擊殘跡之形成與特性。警學叢刊,26(5)=105,47-65。new window  延伸查詢new window
4.Steinberg, M.、Leist, Y.、Goldschmidt, P.、Tassa, M.(1984)。Spectrophotometric Determination of Nitrites in Gunpowder Residue on Shooters' Hands。Forensic Sci,29,464-470。  new window
5.Maloney, R. S.、Thornton, J. I.(1982)。Color test for diphenylamine stabilizer and related compounds in smokeless gunpowder。Journal of Forensic Sciences,27(2),318-329。  new window
6.Kohlbeck, J. A.(1965)。Determinaiton of Nitroglycerin and Resorcinol in Double-Base Propellant Following Separation by Thin Layer Chromatography。Analytical Chemistry,37,1282-1283。  new window
7.Mache, G. F.(1968)。Thin-layer chromatographic/spectrophotometric analysis of certain components in aged double-base propellant。J. Chromatogra,38,47-53。  new window
8.Booker, J. L.(1973)。A method for the identification of smokeless powders and their residues by thin-layer chromatography of their minor constituents。J. Forensic Sci. So,13,199-201。  new window
9.Archer, A. W.(1975)。Separation and identification of minor components in smokeless powders by thin-layer chromatography。Journal of Chromatography,108,401-404。  new window
10.Peak, S. A.(1980)。A thin-layer chromatographic procedure for confirming the presence and identity of smokeless powder flakes。J. Forensic Sci,25(3),679-681。  new window
11.Douse, J. M. F.(1982)。Trace analysis of explosives in handswabs extracts using Amberlite XAD-7 porous polymer beads, silica capillary column gas chromatography with electron-capture detection and thin-layer chromatography。J. Chromatogra,234,415-425。  new window
12.Espinoza, E. O. N.、Thornton, J. I.(1994)。Characterization of smokeless gunpowder by means of diphenylamine stabilizer and its nitrated derivatives。Analytica Chimica Acta,288,57-69。  new window
13.Mach, M. H.、Pallos, A.、Jones, P. F.(1978)。Feasibility of Gunshot Residue Detection Via Its Organic Constituents。Part I: Analysis of Smokeless Powders by Combined Gas Chromatography-Chemical Ionization Mass Spectrometry. J. Forensic Sci,23,433-445。  new window
14.Lloyd, J. B. F.(1986)。Liquid chromatography of firearms propellant traces。J. Energetic Materials,4,239-271。  new window
會議論文
1.Jane, I.、Brooks, P. G.、Douse, J. M. F.、O'Callaghan, K. A.(1983)。Detection of Gunshot Residue via Analysis of Their Organic Constituents475。  new window
圖書
1.Yinon, J.、Zitrin, S.(1981)。The Analysis of Explosives。Pergamon Press。  new window
2.Haslam, J.、Wallis, H. A.、Sguirrell, D. C. M.(1972)。Identification and Analysis of Plastics。Butterworth。  new window
 
 
 
 
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